Boiling Point Determination
A sample in a fusion tube is attached to a thermometer with a rubber band, and immersed in the tube. A sealed capillary, open end pointing down, is placed in the fusion tube. The Thiele tube is heated; dissolved gases evolve from the sample first. Once the sample starts to boil, heating is stopped, and the temperature starts to fall. The temperature at which the liquid sample is sucked into the sealed capillary is the boiling point of the sample.
Read more about this topic: Thiele Tube
Famous quotes containing the words boiling and/or point:
“Twas like a Maelstrom, with a notch,
That nearer, every Day,
Kept narrowing its boiling Wheel”
—Emily Dickinson (18301886)
“No one can doubt the purpose for which the Nation now seeks to use the Democratic Party. It seeks to use it to interpret a change in its own plans and point of view.”
—Woodrow Wilson (18561924)