Cooling Bath

In organic chemistry, a cooling bath is a liquid mixture which is used to maintain low temperatures, typically between 13 °C and -196 °C. These low temperatures are used to collect organic liquids after distillation, to remove solvents using a rotary evaporator, or to perform a chemical reaction below room temperature (see: kinetic control). The cooling agents used in these baths include dry ice, liquid nitrogen, and water ice.

Ethylene glycol baths (% by volume)
Cooling agent Ethylene glycol Ethanol Temp (°C)
Dry ice 0% 100% -78
Dry ice 10% 90% -76
Dry ice 20% 80% -72
Dry ice 30% 70% -66
Dry ice 40% 60% -60
Dry ice 50% 50% -52
Dry ice 60% 40% -41
Dry ice 70% 30% -32
Dry ice 80% 20% -28
Dry ice 90% 10% -21
Dry ice 100% 0% -17

Read more about Cooling Bath:  Ethylene Glycol and Ethanol Baths, Traditional Cooling Baths

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