Melting Point Determination
A sample in a sealed capillary, attached to a thermometer with a rubber band, is immersed in the tube. Heating is commenced, and the temperature ranges at which the sample melts can be then be observed. During heating, the point at which melting is observed and the temperature constant is the melting point of the sample. A more modern method uses dedicated equipment, known as a melting point apparatus. A slow heating rate at the melting point is needed in order to get an accurate measurement. Record the temperature on the thermometer when the sample starts to melt and record the temperature again when all of the sample has melted (this gives you the melting point range). The Thiele tube in itself has many applications such as analyzing and synthesizing organic compounds such as aspirin.
Read more about this topic: Thiele Tube
Famous quotes containing the words melting and/or point:
“Pushkin’s composition is first of all and above all a phenomenon of style, and it is from this flowered rim that I have surveyed its seep of Arcadian country, the serpentine gleam of its imported brooks, the miniature blizzards imprisoned in round crystal, and the many-hued levels of literary parody blending in the melting distance.”
—Vladimir Nabokov (1899–1977)
“You should go to picture-galleries and museums of sculpture to be acted upon, and not to express or try to form your own perfectly futile opinion. It makes no difference to you or the world what you may think of any work of art. That is not the question; the point is how it affects you. The picture is the judge of your capacity, not you of its excellence; the world has long ago passed its judgment upon it, and now it is for the work to estimate you.”
—Anna C. Brackett (1836–1911)