Safety
There are hazards associated even with simple operations such as evaporation. These include implosions resulting from use of glassware that contains flaws, such as star-cracks. Explosions may occur from concentrating unstable impurities during evaporation, for example when rotavapping an ethereal solution containing peroxides. This can also occur when taking certain unstable compounds, such as organic azides and acetylides, nitro-containing compounds, molecules with strain energy, etc. to dryness.
Users of rotary evaporation equipment must take precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, or necklaces. Under these circumstances, the winding action of the rotating parts can draw the users into the apparatus resulting in breakage of glassware, burns, and chemical exposure. Extra caution must also be applied to operations with air reactive materials, especially when under vacuum. A leak can draw air into the apparatus and a violent reaction can occur.
Read more about this topic: Rotary Evaporator
Famous quotes containing the word safety:
“I nightly offer up my prayers to the throne of grace for the health and safety of you all, and that we ought all to rely with confidence on the promises of our dear redeemer, and give him our hearts. This is all he requires and all that we can do, and if we sincerely do this, we are sure of salvation through his atonement.”
—Andrew Jackson (17671845)
“A lover is never a completely self-reliant person viewing the world through his own eyes, but a hostage to a certain delusion. He becomes a perjurer, all his thoughts and emotions being directed with reference, not to an accurate and just appraisal of the real world but rather to the safety and exaltation of his loved one, and the madness with which he pursues her, transmogrifying his attention, blinds him like a victim.”
—Alexander Theroux (b. 1940)
“Perhaps having built a barricade when youre sixteen provides you with a sort of safety rail. If youve once taken part in building one, even inadvertently, doesnt its usually latent image reappear like a warning signal whenever youre tempted to join the police, or support any manifestation of Law and Order?”
—Jean Genet (19101986)