Synthesis
Diethyl phthalate is produced by the reaction of phthalic anhydride with ethanol in the presence of a catalytic amount of concentrated sulfuric acid. Phthalic anhydride is produced by either the oxo process or the Ald-Ox process from ethanol and the oxidation of naphthalene or o-xylene. The purity of manufactured phthalate esters is reportedly between 99.70% and 99.97% with the main impurities being isophthalic acid, terephthalic acid, and maleic anhydride.
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